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Beilstein J. Org. Chem. 2015, 11, 972–979, doi:10.3762/bjoc.11.109
Graphical Abstract
Figure 1: TTF-substituted allenes 1–3.
Scheme 1: Synthesis of 3.
Figure 2: (a) ECD spectra of (R)-(−)-3 (3.5 × 10−5 M), (S)-(+)-3 (3.8 × 10−5 M), (R)-(−)-9 (3.0 × 10−5 M), an...
Scheme 2: Synthesis of chiral (R)-PTDPA and (S)-PTDPA.
Figure 3: (a) UV–vis absorption spectra of 3 and PTDTA in CH2Cl2. (b) Normalized ECD spectra of (R)-PTDPA, (S...
Figure 4: CV of 3 (7.8 × 10−4 M) and PTDPA in PhCN.
Figure 5: Electronic spectra of (a) 3 and its cationic species, and (b) PTDPA and its cationic states of PTDP...